Published September Origi- nally approved in Last previous edition approved in as 3. E – 89a (). Annual Book of ASTM Standards. Buy ASTM E TEST METHODS FOR CHEMICAL ANALYSIS OF COPPER ALLOYS from SAI Global. These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for.
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ASTM E – 03 Standard Test Methods for Chemical Analysis of Copper Alloys
Add 6 to 8 drops of xylenol orange indicator solution and titrate with standard zinc solution until the color changes from yellow to orange or pink. Dilute the aliquot to mL and proceed as directed in AAB 1 2 The precipitate is dissolved in hydrochloric acid and the tin is reduced with iron and nickel and titrated with a standard 4e78 iodate solution in an inert atmosphere. Then add acetic acid dropwise until the color just turns from red to yellow. Draw off and discard the aqueous layer.
Add 8 mL of the DDC solution for each 0.
For low levels of lead, expanded scale readout is advisable. Silicon bronze NIST a 0.
Standard Test Methods for Chemical Analysis of Copper Alloys
Boil the solution gently for 45 min. Iron by the 1,Phenanthroline Photometric Test Method [0. Both areas are exclusive of the stem.
Repeat at least twice with no change in parameters. Using indicator paper, check the pH, which should be between 6. A sensitivity of 0. Dilute to 1 L with water. Cool, dilute to volume, and mix. Users are sstm to employ suitable reference materials, if available to verify the accuracy of the method in their laboratories. The data are summarized in Table The preparation, qstm, and use of KCN solutions require care and attention.
Titrate dropwise until the color changes from purplish-red to yellow. Contamination of the calibration or test solutions by halides may lead to the loss of silver. Using the test cell, take photometric readings of the calibration solutions.
Retain the organic layer. Prepare fresh as needed.
ASTM E478 – 08(2017)
Cover the beaker with a raised cover glass, and evaporate the solution to a volume of 2 to 3 mL. Summary of Test Method Make further additions of formaldehyde and each time titrate to the blue end point to ensure that all the zinc has been released.
Significance and Use These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for compliance with compositional specifications. Add 10 mL of HCl and dilute to 1 L. The percent variability for the highest calibration solution should e47 less than 1.
The actual limits of application of each test method are presented in 1. E has been replaced aztm Practice E As the voice of the U. Repeat this extraction until no further precipitation occurs. Users are encouraged to use this or similar reference materials to verify that the method is performing accurately in their laboratories.